Atlas Volumetric

Atlas Volumetric

Atlas Volumetric

    Atlas Gravimetric Dosing

    Based on an Atlas Potassium, the Atlas Volumetric Dosing System includes an Atlas Syringe Pump or Atlas Syringe Pump XL. The Atlas Syringe Pump is a versatile volumetric dosing and/or sampling system.

    It allows 2 independent refilling flows, one continuous flow, reaction sampling, intelligent control of pH and temperature dependant dosing. It consists of two syringes and multi port valves and can be controlled from the front panel, by the Reactor Master, an Atlas Base or PC software.

    For a schematic of possible dosing modes please refer to the info tab.

    Atlas Syringe Pump Features:

    The pump can be used on its own, connected to a Reactor Master, an Atlas Base or controlled by a PC. In all modes, the two syringes (with up to 6 port valves) can be configured into a variety of configurations. As each port can be used to aspirate from or dispense to, the pump can be used as “one to many”, “many to one”, an autosampler or one continuous flow.The pump can be connected to Atlas pH or temperature sensors to allow control of pumping based on these values. When connected to a Reactor Master or an Atlas Base, reagents can be added automatically after a temperature and stirrer speed has been reached or paused in the case of an exotherm.

    Specifications

    Working Volume Options: 50ml, 100ml, 250ml, 500ml, 1 litre, 2 litres, 3 litres or 5 litres (vessels are interchangeable). Note that vessels greater than 2 litres also require the Remote Mount.
    Reaction Vessel Profile Options: Round bottom, torispherical or conical. Custom available on request.
    Stirrer Options: Anchor, pitched blade propeller, retreat curve (in glass or PTFE), custom available on request.
    Chemical Resistance: All wetted parts made from glass and PTFE (or other similar fluoropolymers)
    Maximum Temperature: +200°C (+250°C with High Temperature Upgrade Kit). The maximum temperature achievable is also circulator dependent.
    Minimum Temperature: -80°C. The minimum temperature achievable is also circulator dependent.
    Temperature Accuracy: Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature.
    Pressure: Vacuum (50mbar) to 0.5 bar (see Atlas Pressure Systems for high pressure).
    Overhead Stirring: Scorpion Overhead Stirrer to 800RPM with 11Ncm Torque (High torque options available to 180Ncm peak, 90Ncm continuous with speed of 1000RPM and torque feedback).
       
    Atlas Syringe Pump  
    Chemical Resistance: All wetted parts are made from glass, PTFE and PCTFE.
    Maximum Pressure: 6 bar.
    Number of Syringes: 2.
    Options for Syringe Sizes: 50ul, 100ul, 250ul, 500ul, 1ml, 2.5ml, 5ml.
    Options for Number of Ports per Valve: 2, 3, 4 or 6.
    Maximum Flow Rate in Continuous Mode: 20% of syringe volume per minute (e.g. 10ul/min when using 50ul syringes)
    Maximum Flow Rate in Dual Dosing Mode: 1% of syringe volume per minute (e.g. 0.5ul/min using a 50ul syringe)
    Maximum Flow Rate in Continuous Mode: 400% of syringe volume (e.g. 20ml/min with 5ml). Note that much higher rates are possible with the Atlas Pressurized Input Store.
    Maximum Flow Rate in Dual Dosing Mode: 400% of syringe volume (e.g. 20ml/min with 5ml). Note that much higher rates are possible with the Atlas Pressurized Input Store.
    Modes of Operation There are 5 main modes of operation (standalone modes shown by *)
      1) Dual Dosing* Dose a volume, pump at a flow rate, dose one reagent to reactors or sophisticated profiles. Connect an Atlas Temperature Probe and Node to pause the addition if over/under temperature.
      2) PH Control* Connect an Atlas pH Probe and Node to dose an acid and/or base to keep within a defined range.
      3) Continuous* 2 syringe pumps work together to produce 1 continuous flow, i.e. one is refilling while the other is dispensing.
      4) Atlas Base Control Atlas Syringe Pump can be controlled from the Base Unit as part of an automated temperature and stirrer speed profile.
      5) PC Control PC software can control Dual Dosing and pH Control in the same way as the Atlas Syringe Pump.

     

    System Details
    Stirrer - PTFE 4 Blade Propeller 300mm x 40mm dia
    Stirrer - PTFE 4 Blade Propeller 400mm x 40mm dia
    Stirrer - PTFE 4 Blade Propellor 500mm x 40mm dia
    Stirrer - PTFE Anchor 300mm x 80mm dia
    Stirrer - PTFE Anchor 400mm x 80mm dia
    Stirrer - PTFE 2 Blade Centrifugal 300mm
    Scorpion Overhead Stirrer
    Support Rods (Pack of 2)
    Stirrer Seal and Guide
    Jacketed Vessel Clamp
    Oil Drain Unit
    Oil Pipes from Reactor to Oil Drain Unit (Pack of 2)
    Oil Pipes from Circulator to Oil Drain Unit (Pack of 2)
    Temperature Node
    Node Extension
    Triple Node Socket
    Jacket Vessel Lid (UK & EU)
    Reaction Vessel Drip Tray
    Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 45mm dia
    Jacketed Vessel 100 ml Round Bottom
    Jacketed Vessel 250 ml Round Bottom
    Jacketed Vessel 500 ml Round Bottom
    Jacketed Vessel 1 litre Round Bottom
    Jacketed Vessel 2 litre Round Bottom
    Reaction Vessel Seal (FFKM)
    6mm Dia RTD Probe Holder
    8mm Dia RTD Probe Holder
    RTD Probe - PTFE Coated 200mm x 6mm
    RTD Probe - PTFE Coated 300mm x 8mm
    RTD Probe - PTFE Coated 400mm x 8mm
    Stirrer - PTFE 3 Blade Retreat Impeller 400mm x 75mm dia
    RTD Probe - PTFE Coated 100mm x 6mm
    Jacketed Vessel Lid (US)
    Circulator (Julabo CF40) 115V / 60HZ
    Gold Cold Circulator (Julabo FP51-SL) 230V / 60Hz / 3Phase
    Circulator (Julabo CF40) 230V / 50HZ
    Gold Cold Circulator (Julabo FP51-SL) 400VC / 50Hz / 3Phase
    Atlas Syringe Pump
    Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 75mm dia
    Stirrer - PTFE Anchor 500mm x 80mm dia
    Atlas Syringe Pump - without Valves or Syringes
    RTD Probe - PTFE Coated 500mm x 9mm
    Stirrer - PTFE 3 Blade Retreat Impeller 500mm x 75mm dia
    Julabo Circulator Fluid (+20 to +250C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-50 to +105C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-20 to +180C) for Open Baths, 10 Litres
    Stirrer - PTFE 3 Blade Retreat Impeller 650mm x 75mm dia
    Circulator (Julabo CF40) 100V / 60Hz
    Bronze Circulator (Julabo CF41) 115V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 50Hz
    Copper Circulator (Julabo CF30) 100V / 60Hz
    Copper Circulator (Julabo CF30) 115V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 50Hz
    Jacketed Vessel 5 litre Round Bottom
    Jacketed Vessel 3 litre Round Bottom
    RTD Probe - PTFE Coated 600mm x 9mm
    Stirrer - Glass Anchor 300mm x 36mm
    Asia Pump (2 Channels, No Syringes)
    Atlas XL Syringe Pump - without Valves or Syringes
    Huber Circulator - Unistat Petite Fleur (230V 1Ph 50Hz)
    Atlas XL Syringe Pump
    Huber Circulator - Unistat 705 (230V 1Ph 50Hz)
    Huber Circulator - Unistat 705 (208V 2Ph 60Hz)
    Huber Circulator - Unistat Tango Nuevo (230V 1Ph 50Hz)
    Huber Circulator - Unistat Tango Nuevo (208V 2Ph 60Hz)
    Huber Circulator - Unistat Petite Fleur (115V 1Ph 60Hz)
    Huber Circulator - CC510 (400V 3Ph 50Hz)
    Huber Circulator - CC510 (208V 2Ph 60Hz)
    Huber Circulator - CC505 (230V 1Ph 50Hz)
    Huber Circulator - CC505 (208V 2Ph 60Hz)
    Huber Circulator - Ministat 240-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 230-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 125-cc (230V 1Ph 50Hz)
    Huber Circulator - Unistat Petite Fleur (208V 2Ph 60Hz)
    Huber Circulator - Ministat 230-cc (115V 1Ph 60Hz)
    Huber Circulator - Ministat 125-cc (100-115V 1Ph 50-60Hz)
    Julabo Circulator Fluid (-40 to +250C) Closed Bath Presto, 10 Litres
    Julabo Circulator Fluid (-85 to +170C) Closed Bath Presto, 10 Litres
    Huber Circulator Fluid (-60 to +115C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-40 to +165C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-20 to +235C [Closed]/+195C [Open]), 10 Litres
    Huber Circulator Fluid (+20 to +275C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid DW-Therm (-90 to +200C) for Closed Units, 10 Litres
    Silver Circulator (Julabo FP50-HL) 230V / 50Hz
    Silver Circulator (Julabo FP50-HL) 230V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 60Hz
    Circulator (Julabo CF40) 230V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 60Hz
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (UK Plug)
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (EU Plug)
    Gold Circulator (Julabo Presto A40) 208V 60Hz (US Plug)
    5L Jacketed Vessel Round Bottom (Requires Globe Offset Assembly 2200636)
    Huber E-Grade Exclusive Upgrade for Ministat and CC (9495)
    PTFE Anchor 600mm x 80mm dia
    PTFE 4 Blade Propellor 600mm x 60mm dia
    Base to Circulator Serial Cable (RJ11 to DB9 Male)
    Overflow Displacement Tank - Ministat 125
    Overflow Displacement Tank - Ministat 230
    Overflow Displacement Tank - Ministat 240

    Downloads

      Name Type Format Language Download
    Atlas Syringe Pump Brochure Brochure PDF en Link to file
    Atlas Brochure Brochure PDF en Link to file
    Syrris Batch Chemistry Reactors Catalogue PDF en Link to file
    Atlas Potassium Flyer PDF en Link to file
    Atlas Syringe Pump Flyer PDF en Link to file
    Atlas Overview Video MOV en View

     

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    Contact

    • Marc Ujma
    • Product Specialist Synthesis
    • ph. +49 (0)2064 427-281