Atlas Sodium High Pressure

Atlas Sodium High Pressure

Atlas Sodium High Pressure

    Atlas Sodium High Pressure

    The Atlas Sodium Pressure System is designed for applications where elevated pressures (up to 200 bar) or temperatures (Hotplate temperatures up to 350 ºC) are required e.g. hydrogenations, carbonylations, etc.

    The easy to use modular pressure reactor system can be controlled manually or automatically using the intuitive control knob and/or Atlas Software. Available in volumes of 100, 160, 300 and 450 ml in stainless steel 316, hastelloy, titanium, etc., the Atlas Sodium Pressure System offers heating and/or cooling, overhead stirring (to 800 RPM) or magnetic stirring (to 1200 RPM).

    The reactor (shown opposite) includes a dip tube for sampling, a cooling coil, a thermowell, an impellor, valves, a manual pressure gauge and burst disc to ensure safe operation.

    The basic system allows automatic temperature and stirrer control and pressure sensing. Upgrades include a pressure node and sensor for pressure logging, Gas Selection Module, Pressure Control Module, gas flow meters and full PC software control and automation. For more information, please contact Syrris.

     

    Benefits and Specifications:

    High pressure: The Atlas Sodium Pressure System has an operating pressure of up to 200 bar (contact Syrris for higher pressures).
    Easy to use: Dry Bath for high pressure reactor is designed to fit easily and safely on the Atlas hotplate.
    Advanced control: The PC software offers gas selection and automated pressure or mass flow control.
    High performance stirring: The Atlas Sodium Pressure System offers powerful overhead (up to 800RPM) or magnetic stirring (up to 1200RPM).
    Versatile: The Atlas Sodium Pressure System offers liquid sampling at high pressures/temperatures.
    Ideal for catalyst screening: Quick automation and optimisation of high pressure reactions.
    Variety of vessels: The Atlas Sodium Pressure System can be supplied with 100, 160, 300 and 450ml reaction vessels in stainless steel 316, hastelloy, titanium, etc.
    Safe: Burst disc, maximum temperature cut out and complies with PED / ASME design codes.
    Data-logging without PC Software: All data such as pressure, temperature, stirrer speed, etc. is logged automatically.

     

    Specifications

    Safety: Burst disc.
    Working Volume Options: 100ml, 160ml, 300ml or 450ml.
    Stirrer: Pitched blade propeller. Custom available on request.
    Chemical Resistance: All wetted parts are made from Stainless Steel 316 (Hastelloy also available).
    Maximum Temperature: +280°C hotplate temperature (350°C hotplate temperature with hotter hotplate).
    Minimum Temperature: Room temperature (-40°C cold plate temperature with Hot and Cold Plate).
    Temperature Accuracy: Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature.
    Pressure: Vacuum (50mbar) to 0.5 bar (see Atlas Pressure Systems for high pressure).
    Overhead Stirring: Scorpion Overhead Stirrer to 800RPM with 11Ncm Torque (High torque options available to 180Ncm peak, 90Ncm continuous with speed of 1000RPM and torque feedback).
    Modes of Operation: Manual (set on Atlas Base), Automated (set on Atlas Base) or full PC Software control.
    Liquid Sampling: Possible using valve and dip tube.

     

    System Details
    Hotplate (230V)
    Scorpion Overhead Stirrer
    Hotplate (120V)
    Support Rods (Pack of 2)
    Port
    Temperature Node
    Drybath for 100ml High Pressure Vessel
    Drybath for 160ml High Pressure Vessel
    Drybath for 300ml High Pressure Vessel
    Drybath for 450ml High Pressure Vessel
    High Pressure Vessel Lid T316SS, Overhead Stirrer Adaptor (Max Temp 275oC)
    High Pressure Vessel T316SS - 160ml, Dip Tube, Coil, Thermowell and Impellor
    High Pressure Vessel T316SS - 300ml, Dip Tube, Coil, Thermowell and Impellor
    High Pressure Vessel T316SS - 450ml, Dip Tube, Coil, Thermowell and Impellor
    Aalborg Mass Flow Meter 0-10L/min
    Alborg Mass Flow Controller
    Gas Selection Module
    200 Bar Gas Pressure Control Module (100 Bar with H2)
    Hotter Hotplate (to 350C) 240V
    High Pressure Vessel T316SS - 100ml, Dip Tube, Coil, Thermowell and Impellor
    High Pressure Vessel Lid Hastelloy C276, Overhead Stirrer Adaptor (Max Temp 275oC)
    High Pressure Vessel Hastelloy C276 - 100ml, Dip Tube, Coil, T-well and Impellor
    High Pressure Vessel Hastelloy C276 - 160ml, Dip Tube, Coil, T-well and Impellor
    High Pressure Vessel Hastelloy C276 - 300ml, Dip Tube, Coil, T-well and Impellor
    High Pressure Vessel Hastelloy C276 - 450ml, Dip Tube, Coil, T-well and Impellor
    Hotter Hotplate (to 350C) 120V
    High Pressure Vessel Lid T316SS, No Overhead Stirrer Adapter (Max Temp 275oC))
    High Pressure Vessel Lid Hastelloy C276, No Overhead Stirrer Adapter (Max Temp 275oC)
    High Pressure Vessel PED Certification (required for all EU systems)
    High Pressure Vessel ASME Certification
    High Pressure Vessel Lid T316SS, Overhead Stirrer Adapter (Max Temp 350oC)
    High Pressure Vessel Lid T316SS, No Overhead Stirrer Adapter (Max Temp 350oC)
    High Pressure Vessel Lid Hastelloy, Overhead Stirrer Adapter (Max Temp 350oC)
    High Pressure Vessel Lid Hastelloy, No Overhead Stirrer Adapter (Max Temp 350oC)
    Stainless Steel 3mm diameter RTD probe for 100ml and 160ml High Pressure Reactors
    Stainless Steel 3mm diameter RTD probe for 300ml High Pressure Reactor
    Stainless Steel 3mm diameter RTD probe for 450ml High Pressure Reactor
    Atlas Software 1
    200 Bar System Starter Kit (Selection of Pipes and Fittings)
    Pressure Node for 200 Bar System
    Pressure Sensor for 200 Bar System

    Downloads

      Name Type Format Language Download
    Atlas Brochure Brochure PDF E Link to file
    Syrris Batch Chemistry Reactors Catalogue PDF E Link to file
    Atlas High Pressure Na Flyer PDF E Link to file
    Atlas Potassium Pressure Flyer PDF en Link to file
    Atlas Jacketed Reactors Video MOV en View
    Atlas Overview Video MOV en View

     

    Related Categories

    Contact

    • Marc Ujma
    • Product Specialist Synthesis
    • ph. +49 (0)2064 427-281