Atlas Potassium Pressure

Atlas Potassium Pressure

Atlas Potassium Pressure

    Atlas Potassium Pressure

    The Atlas Potassium Pressure System is a modular 3 bar pressure reactor system that can be controlled automatically or manually. It is available with reactors in volumes of 100ml, 250ml, 500ml, 1L, 2L or 3L (single or vacuum jacketed) that can be changed in under a minute without the need for tools.

    The Atlas Potassium Pressure System is designed for applications where elevated pressures are required e.g. hydrogenations, carbonylations etc. or high vacuum applications. The basic system allows automatic temperature control (-80°C to +200°C*) and stirrer control (up to 800RPM or 2000RPM) and pressure sensing. This data is also displayed and automatically logged by the base. The system includes a burst disc and pressure relief valve.

    Upgrades include the Gas Selection Module, Pressure Control Module, gas flow meters/controllers and full PC software control and automation. For more information, please contact Syrris.

     

    Benefits

    Quick change vessel: The oil drain unit, jacketed vessel clamp and quick oil connectors allow vessels to be changed in under a minute.
    Easy to use: No tools required, twist and click control knob, large display and intuitive.
    High performance stirring: The Atlas Potassium Pressure System offers powerful overhead stirring.
    3 bar pressure: The Atlas Potassium Pressure System has an operating pressure of up to 3 bar (see the Custom Reactor Systems for higher pressure).
    Variety of vessels: The Atlas Potassium Pressure System can be supplied with 100ml, 250ml, 500ml, 1L, 2L or 3L glass reaction vessels with or without vacuum jacket.
    Safe: Burst disc, pressure relief valve and complies with PED / ASME design codes.
    Automation and data-logging without PC: Automatic profiles are possible for reaction temperature, stirrer speed, reagent addition and sampling. All data is logged in a .csv file and can be downloaded to a USB stick automatically.
    Optional PC control: The PC software offers advanced recipe control, total automation of all parameters, alarms and real time graphs.
    Wide temperature range: -80 to +200°C.

     

     

    Atlas Potassium Pressure System features

    The Atlas Potassium Pressure System is designed for applications where elevated pressures are required e.g. hydrogenations, carbonylations, etc. The basic system, allows automatic temperature and stirrer control and pressure sensing. Upgrades include the Gas Selection Module, Pressure Control Module, gas flow meters and full PC software control and automation. For more information, please contact Syrris.

     

    Modes of operation

    Manual Pressure Control

    Use the Atlas Pressure Node and Sensor with manual valves to control pressure. Pressure, temperature and stirrer speed are displayed and logged automatically.

     

    Automatically Maintain a Pressure

    By using the Atlas Pressure Control Module a consistent pressure to the reaction is maintained over the reaction period and can automatically vent in the case of over pressure. This module also offers, Vent and Purge options.

     

    Pressure Control with Mass Flow Monitoring

    Maintain a pressure and monitor mass flow. Ideal for gas uptake monitoring.

     

    Mass Flow Control

    Dose a known quantity of gas using the mass flow controller.

     

    Off Gas Monitoring

    Monitor off-gases with mass flow meters.

     

    *Manual or Automated Gas Selection
    All of the above modes of operation are available with the Atlas Gas Selection Module, allowing manual or automated selection of up to 3 gases.

    Specifications

    Working Volume Options: 100ml, 250ml, 500ml, 1 litre, 2 litres or 3 litres (vessels are interchangeable and available with or without vacuum jacket). Note that larger vessels also require the Remote Mount.
    Reaction Vessel Profile Options: Round bottom. Custom available on request.
    Stirrer Options: Anchor, pitched blade propeller, retreat curve (in glass or PTFE), custom available on request.
    Maximum Temperature: +200°C. The maximum temperature achievable is also circulator dependent.
    Minimum Temperature: -80°C. The minimum temperature achievable is also circulator dependent.
    Temperature Accuracy: Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature.
    Pressure: Vacuum (50mbar) to 3 bar (see Custom Reactor Systems for high pressure).
    Overhead Stirring: Scorpion Overhead Stirrer to 800RPM with 11Ncm Torque (High torque options available to 180Ncm peak, 90Ncm continuous with speed of 1000RPM and torque feedback).
    Levels of Automation: Manual (set on Atlas Base), Automated (set on Atlas Base) or full PC Software control.
    Safety: Reaction calorimetry, automated liquid dosing, FTIR analysis, reaction sampling, pH analysis and control etc.
    Upgrade options include: Reaction calorimetry, automated liquid dosing, FTIR analysis, reaction sampling, pH analysis and control etc.

     

    System Details
    Scorpion Overhead Stirrer
    Port
    Temperature Node
    Node Extension
    Triple Node Socket
    Standard Solid Phase Reactor Size 1 (3mm ID)
    RTD Probe - PTFE Coated 200mm x 6mm
    RTD Probe - PTFE Coated 300mm x 8mm
    RTD Probe - PTFE Coated 400mm x 8mm
    RTD Probe - PTFE Coated 100mm x 6mm
    Gold Cold Circulator (Julabo FP51-SL) 230V / 60Hz / 3Phase
    Circulator (Julabo CF40) 230V / 50HZ
    Gold Cold Circulator (Julabo FP51-SL) 400VC / 50Hz / 3Phase
    Atlas Syringe Pump
    Atlas Syringe Pump - without Valves or Syringes
    RTD Probe - PTFE Coated 500mm x 9mm
    Julabo Circulator Fluid (+20 to +250C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-50 to +105C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-20 to +180C) for Open Baths, 10 Litres
    Baffles for 1 litre Torispherical Jacketed Vessel (Pack of 2)
    Circulator (Julabo CF40) 100V / 60Hz
    Bronze Circulator (Julabo CF41) 115V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 50Hz
    Copper Circulator (Julabo CF30) 100V / 60Hz
    Copper Circulator (Julabo CF30) 115V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 50Hz
    RTD Probe - PTFE Coated 600mm x 9mm
    Atlas XL Syringe Pump - without Valves or Syringes
    Jacketed Vessel 1 Ltr Round Bottom (Rated to 3 Bar)
    Jacketed Vessel 500ml Round Bottom (Rated to 3 Bar)
    Stirrer Seal and Guide Stainless Steel (3 Bar System)
    Aalborg Mass Flow Meter 0-10L/min
    Alborg Mass Flow Controller
    Huber Circulator - Unistat Petite Fleur (230V 1Ph 50Hz)
    Pressure Sensor
    Atlas XL Syringe Pump
    Stirrer Seal and Guide PTFE (3 Bar System)
    Jacketed Vessel 100ml Round Bottom (Rated to 3 Bar)
    Jacketed Vessel 250ml Round Bottom (Rated to 3 Bar)
    Jacketed Vessel 2 Ltr Round Bottom (Rated to 3 Bar)
    Jacketed Vessel 3 Ltr Round Bottom (Rated to 3 Bar)
    Anchor Stirrer PTFE (500ml to 3 litre Vessels) Cut to Length (3 Bar System)
    Anchor Stirrer Glass (100ml to 250ml Vessels) Cut to Length (3 Bar System)
    Anchor Stirrer Glass (500ml to 3 litre Vessels) Cut to Length (3 Bar System)
    4 Blade Propeller Stirrer PTFE Cut to Length (3 Bar System)
    4 Blade Propeller Stirrer Glass Cut to Length (3 Bar System)
    Retreat Curve Stirrer PTFE (500ml to 3 litre Vessels) Cut to Length (3 Bar System)
    Retreat Curve Stirrer Glass (100ml to 250ml Vessels) Cut to Length (3 Bar System)
    Retreat Curve Stirrer Glass (500ml to 3 litre Vessels) Cut to Length (3 Bar System)
    6mm Probe Holder (3 Bar System)
    8mm Probe Holder (3 Bar System)
    9mm Probe Holder (3 Bar System)
    Quick Response RTD Probe Holder (3 Bar System)
    Calorimetry Heater Probe Holder (3 Bar System)
    Huber Circulator - Unistat 705 (230V 1Ph 50Hz)
    Huber Circulator - Unistat 705 (208V 2Ph 60Hz)
    Huber Circulator - Unistat Tango Nuevo (230V 1Ph 50Hz)
    Huber Circulator - Unistat Tango Nuevo (208V 2Ph 60Hz)
    Huber Circulator - Unistat Petite Fleur (115V 1Ph 60Hz)
    Huber Circulator - CC510 (400V 3Ph 50Hz)
    Huber Circulator - CC510 (208V 2Ph 60Hz)
    Huber Circulator - CC505 (230V 1Ph 50Hz)
    Huber Circulator - CC505 (208V 2Ph 60Hz)
    Huber Circulator - Ministat 240-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 230-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 125-cc (230V 1Ph 50Hz)
    Huber Circulator - Unistat Petite Fleur (208V 2Ph 60Hz)
    Huber Circulator - Ministat 230-cc (115V 1Ph 60Hz)
    Huber Circulator - Ministat 125-cc (100-115V 1Ph 50-60Hz)
    Julabo Circulator Fluid (-40 to +250C) Closed Bath Presto, 10 Litres
    Julabo Circulator Fluid (-85 to +170C) Closed Bath Presto, 10 Litres
    Huber Circulator Fluid (-60 to +115C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-40 to +165C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-20 to +235C [Closed]/+195C [Open]), 10 Litres
    Huber Circulator Fluid (+20 to +275C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid DW-Therm (-90 to +200C) for Closed Units, 10 Litres
    3 Bar Gas Pressure Control Module
    Silver Circulator (Julabo FP50-HL) 230V / 50Hz
    Silver Circulator (Julabo FP50-HL) 230V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 60Hz
    Circulator (Julabo CF40) 230V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 60Hz
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (UK Plug)
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (EU Plug)
    Gold Circulator (Julabo Presto A40) 208V 60Hz (US Plug)
    Huber E-Grade Exclusive Upgrade for Ministat and CC (9495)
    Atlas Software 1
    Overflow Displacement Tank - Ministat 125
    Overflow Displacement Tank - Ministat 230
    Overflow Displacement Tank - Ministat 240
    Pressure Node for 3 Bar System

    Downloads

      Name Type Format Language Download
    Atlas Brochure Brochure PDF E  
    Syrris Batch Chemistry Reactors Catalogue PDF E  
    Atlas Potassium Pressure Flyer PDF E  
    Atlas Jacketed Reactors Video MOV E View
    Atlas Overview Video MOV E View

     

    Related Categories

    Contact

    • Marc Ujma
    • Product Specialist Synthesis
    • ph. +49 (0)2064 427-281