Atlas Calorimeter

Atlas Calorimeter

Atlas Calorimeter

    Atlas Reaction Calorimeter

    The Atlas Calorimeter is an easy-to-use, high performance system. Using either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), Atlas can generate power and enthalpy graphs quickly and easily.

    This, combined with the simple configuration of reaction temperatures, dosing quantities and alarms provides chemistry laboratories with an easy, safe and accurate calorimetry system. Based on the standard Atlas Potassium, the Atlas Calorimeter also includes a power supply and the intelligent Atlas Software that can create graphs within seconds.

    For more information on the Atlas Calorimeter, please watch the video below. For those without sound, English subtitles are included by default.

     

    Watch the Atlas Calorimeter Video

    Watch the Atlas Calorimeter Video [see more videos...]

    Benefits and Specifications:

    • Fully automated: Temperature control, set up and operation are all automated.
    • Excellent control:Sophisticated PID control and  powerful circulators result in accurate isothermal performance.
    • Accurate:Vacuum jacketed vessels, automated calibration and sensitive RTDs give extremely high accuracy results.
    • Walk away operation: Automated gravimetric or volumetric reagents additions are all made easy.
    • High performance overhead stirrer:Improved formulation consistency, stability and performance of final drug products.
    • Easy analysis:Easy to use software allows graphs of power and enthalpy to be plotted with one click.
    • Quick:Everything clicks together quickly and easily without the need for tools. Vessels can be changed in under 1 minute.
    • Flexible:The same equipment and software can be used for HFC or PCC, allowing the chemist to pick the best method for the reaction.

     

    Atlas HFC and PCC System features:

    Atlas PC Software offers truly easy calorimetry operation. Configuration of parameters such as reaction temperature, dosing quantities, expected power level (e.g. moderate endotherm; strong exotherm) and alarms (with subsequent actions) are defined in an easy to use wizard.

    When running the experiment, everything is controlled automatically including stabilization at desired reaction temperature, reagent addition and in the case of HFC, pre and/or post run calibration. No user intervention is required during the entire process. All data is continually logged to a common csv file and displayed by the software in graph format in real time.

    The software automatically includes the calibration, compensates for the enthalpy of addition and deviations from isothermal conditions. Analysis is made easy by the Atlas Software featuring “single click” plotting of power and enthalpy.

     

    Specifications

    Interchangeable Jacketed Reaction Vessels: 100ml, 250ml, 500ml, 1 litre and 2 litre vacuum jacketed reactors available with a range of profiles including round, torispherical, conical or custom.
    Temperature Range: -40°C to 150°C recommended for calorimetry (up to 200°C possible).
    Accuracy: Typically 1 to 5% (dependent on settling time and external conditions).
    Calorimetric Techniques Used: Heat flow calorimetry (HFC) or power compensation calorimetry (PCC).
    Footprint: From 40cm (16”) wide.
    Chemical Resistance: Glass, PTFE and other fluoropolymers.
    Maximum Reaction Power: 100W/litre maximum (50W for power compensation calorimetry).
    Safety Features: Warnings, alarms and automatic shutdown can be set for the whole experiment and each process step.
    Stirring Options: Anchor, pitched blade propeller, retreat curve impeller or custom made in glass or PTFE. 0-800RPM (up to 11Ncm) or 0-1000RPM (up to 90Ncm) with torque feedback.
    Circulator Options: Julabo, Huber, Lauda, Haake
    Equipment Supplied:

    Atlas Calorimetry Software Upgrade and Atlas Reporting Software

    Atlas Port for recirculator control

    Vacuum jacketed vessel (see above)

    Fast response reaction temperature probe

    Tj (jacket in) measurement probe with node and insulated cover

    PC controlled heater power supply with Atlas Port

    Reactor heater

    Dosing Options: Manual dosing, Atlas Syringe Pump for automatic volumetric dosing or peristaltic pump and balance for gravimetric dosing.
    Other Sensor Options: pH, in-situ FTIR sensor, turbidity, pressure, etc.

     

    System Details
    Stirrer - PTFE 4 Blade Propeller 300mm x 40mm dia
    Stirrer - PTFE 4 Blade Propeller 400mm x 40mm dia
    Stirrer - PTFE 4 Blade Propellor 500mm x 40mm dia
    Stirrer - PTFE Anchor 300mm x 80mm dia
    Stirrer - PTFE Anchor 400mm x 80mm dia
    Stirrer - PTFE 2 Blade Centrifugal 300mm
    Scorpion Overhead Stirrer
    Support Rods (Pack of 2)
    Stirrer Seal and Guide
    Jacketed Vessel Clamp
    Oil Drain Unit
    Oil Pipes from Reactor to Oil Drain Unit (Pack of 2)
    Oil Pipes from Circulator to Oil Drain Unit (Pack of 2)
    Node Extension
    Triple Node Socket
    Jacket Vessel Lid (UK & EU)
    Reaction Vessel Drip Tray
    Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 45mm dia
    Jacketed Vessel 100 ml Round Bottom
    Jacketed Vessel 250 ml Round Bottom
    Jacketed Vessel 500 ml Round Bottom
    Jacketed Vessel 1 litre Round Bottom
    Jacketed Vessel 2 litre Round Bottom
    Reaction Vessel Seal (FFKM)
    6mm Dia RTD Probe Holder
    8mm Dia RTD Probe Holder
    RTD Probe - PTFE Coated 200mm x 6mm
    RTD Probe - PTFE Coated 300mm x 8mm
    RTD Probe - PTFE Coated 400mm x 8mm
    Stirrer - PTFE 3 Blade Retreat Impeller 400mm x 75mm dia
    RTD Probe - PTFE Coated 100mm x 6mm
    Jacketed Vessel Lid (US)
    Circulator (Julabo CF40) 115V / 60HZ
    Gold Cold Circulator (Julabo FP51-SL) 230V / 60Hz / 3Phase
    Circulator (Julabo CF40) 230V / 50HZ
    Gold Cold Circulator (Julabo FP51-SL) 400VC / 50Hz / 3Phase
    pH Probe - 400mm with Swivel Adaptor
    pH and Temperature Node
    Atlas Syringe Pump
    Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 75mm dia
    Stirrer - PTFE Anchor 500mm x 80mm dia
    Atlas Syringe Pump - without Valves or Syringes
    RTD Probe - PTFE Coated 500mm x 9mm
    Stirrer - PTFE 3 Blade Retreat Impeller 500mm x 75mm dia
    Julabo Circulator Fluid (+20 to +250C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-50 to +105C) for Open Baths, 10 Litres
    Julabo Circulator Fluid (-20 to +180C) for Open Baths, 10 Litres
    Stirrer - PTFE 3 Blade Retreat Impeller 650mm x 75mm dia
    Circulator (Julabo CF40) 100V / 60Hz
    Bronze Circulator (Julabo CF41) 115V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 50Hz
    Copper Circulator (Julabo CF30) 100V / 60Hz
    Copper Circulator (Julabo CF30) 115V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 50Hz
    Jacketed Vessel 5 litre Round Bottom
    Jacketed Vessel 3 litre Round Bottom
    RTD Probe - PTFE Coated 600mm x 9mm
    Stirrer - Glass Anchor 300mm x 36mm
    Atlas XL Syringe Pump - without Valves or Syringes
    Huber Circulator - Unistat Petite Fleur (230V 1Ph 50Hz)
    Atlas XL Syringe Pump
    Huber Circulator - Unistat 705 (230V 1Ph 50Hz)
    Huber Circulator - Unistat 705 (208V 2Ph 60Hz)
    Huber Circulator - Unistat Tango Nuevo (230V 1Ph 50Hz)
    Huber Circulator - Unistat Tango Nuevo (208V 2Ph 60Hz)
    Huber Circulator - Unistat Petite Fleur (115V 1Ph 60Hz)
    Huber Circulator - CC510 (400V 3Ph 50Hz)
    Huber Circulator - CC510 (208V 2Ph 60Hz)
    Huber Circulator - CC505 (230V 1Ph 50Hz)
    Huber Circulator - CC505 (208V 2Ph 60Hz)
    Huber Circulator - Ministat 240-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 230-cc (230V 1Ph 50Hz)
    Huber Circulator - Ministat 125-cc (230V 1Ph 50Hz)
    Huber Circulator - Unistat Petite Fleur (208V 2Ph 60Hz)
    Huber Circulator - Ministat 230-cc (115V 1Ph 60Hz)
    Huber Circulator - Ministat 125-cc (100-115V 1Ph 50-60Hz)
    Julabo Circulator Fluid (-40 to +250C) Closed Bath Presto, 10 Litres
    Julabo Circulator Fluid (-85 to +170C) Closed Bath Presto, 10 Litres
    Huber Circulator Fluid (-60 to +115C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-40 to +165C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid (-20 to +235C [Closed]/+195C [Open]), 10 Litres
    Huber Circulator Fluid (+20 to +275C) Open/Closed Units, 10 Litres
    Huber Circulator Fluid DW-Therm (-90 to +200C) for Closed Units, 10 Litres
    Silver Circulator (Julabo FP50-HL) 230V / 50Hz
    Silver Circulator (Julabo FP50-HL) 230V / 60Hz
    Bronze Circulator (Julabo CF41) 230V / 60Hz
    Circulator (Julabo CF40) 230V / 60Hz
    Copper Circulator (Julabo CF30) 230V / 60Hz
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (UK Plug)
    Gold Circulator (Julabo Presto A40) 230V 50/60Hz (EU Plug)
    Gold Circulator (Julabo Presto A40) 208V 60Hz (US Plug)
    5L Jacketed Vessel Round Bottom (Requires Globe Offset Assembly 2200636)
    Huber E-Grade Exclusive Upgrade for Ministat and CC (9495)
    PTFE Anchor 600mm x 80mm dia
    PTFE 4 Blade Propellor 600mm x 60mm dia
    Base to Circulator Serial Cable (RJ11 to DB9 Male)
    Overflow Displacement Tank - Ministat 125
    Overflow Displacement Tank - Ministat 230
    Overflow Displacement Tank - Ministat 240

    Downloads

      Name Type Format Language Download
    Atlas Calorimeter Brochure Brochure PDF E Link to file
    Atlas Brochure Catalogue PDF E Link to file
    Syrris Batch Chemistry Reactors Flyer PDF E Link to file
    Atlas Calorimeter Video MOV E View
    Atlas Jacketed Reactors Video MOV E View
    Atlas Overview Video MOV E View

     

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    Contact

    • Marc Ujma
    • Product Specialist Synthesis
    • ph. +49 (0)2064 427-281